Liz 1,Zhang Yu 1,Zhou Ying 1,Ma Chengliang 1,Huang Wenjiang 1,Ji Chen 2
Abstract:
In this experiment, MoSi2 composite ceramics were prepared by wet-grinding and mixing nano-sized Al2O3 particles of the different volume fractions with Mo powder and Si powder (molybdenum-silicon molar ratio of 1:2), and its physical properties such as density, hardness and fracture toughness were tested. The phase composition, micro-morphology and micro-elemental composition of the prepared samples were analyzed by XRD, SEM and EDS. The effects of nano-Al2O3 particles with the different volume fractions on the properties of MoSi2 composite ceramics were discussed. The results show that: (1) The density, hardness and fracture toughness of MoSi2 can be effectively improved by adding a small amount of nano-Al2O3 compared with a single MoSi2 phase, the density, hardness and fracture toughness of nano-102%, 119% and 167% respectively; (2) Under the vacuum reaction hot-pressing sintering, a small amount of nano-Al2O3 incorporates the lattice distortion of the MoSi2 composite ceramics, which is beneficial to improve the fracture toughness; (3) As the amount of nano-Al2O3 increases, the dispersibility of nano-Al2O3 in the MoSi 2-based material decreases, resulting in the decrease of the physical properties?of the MoSi2 composite ceramic.