CHEN Jun-ying1,FENG Xiang-ying1,2,SHI Zhao-xia’1,3,FANG Shu-qi1,HAN Xiu-li1, WANG Duo1
Abstract:
The activated carbon was prepared from desilicon rice husk by compound activating agents ( NaOHand Na,CO,). The influence of four factors ( activation temperature,activation time,mixed ratio,mass con-centration of the impregnating solution) and three levels w investigated. The process was optimized by re-sponse surface methodology. The results showed that activation temperature and concentration of the impregna-ting solution were important factors on iodine adsorption value of activated carbon. The best conditions of pre-paring activated carbon the activation temperature of 635℃,activation time of 35 min,the mixing ratio of 4 :l,mass concentration of the impregnating solution of 40%.The iodine adsorption value was 1383.5 mg/g,which was consistent with the predicted values. The structure and morphology of samples characterized bySEM. The specific surface area and pore-size distribution calculated by the methods of BET and BJH, respec-tively. The activated rice husk carbon exhibit a high specific surface area of 1566.1m /g,average pore diam-eter of 2. 05 nm ,total pore volume of 0.80 cm’/ g.