[1]ZHOU Cairong,Anna,SHI Xiaohua,et al.Thermal analysis of trans-ferulic acid[J].Journal of Zhengzhou University (Engineering Science),2007,28(02):47-50.[doi:10.3969/j.issn.1671-6833.2007.02.012]
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Journal of Zhengzhou University (Engineering Science)[ISSN
1671-6833/CN
41-1339/T] Volume:
28
Number of periods:
2007年02期
Page number:
47-50
Column:
Public date:
1900-01-01
- Title:
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Thermal analysis of trans-ferulic acid
- Author(s):
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ZHOU Cairong; Anna; SHI Xiaohua; etc
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- Keywords:
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- CLC:
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- DOI:
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10.3969/j.issn.1671-6833.2007.02.012
- Abstract:
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The melting point, heat of melting, decomposition temperature and other properties of trans-ferulic acid were experimentally studied by differential scanning calorimetry and thermogravimetric analysis method, and the conditions for the determination of trans-ferulic acid by DSC-60 differential scanning calorimeter were determined, that is, under the conditions of a heating rate of 10°C·min-1 and a nitrogen flow rate of 20 mL·min-1, the sample could be analyzed to obtain a more accurate DSC curve, and under these conditions, the melting point of trans-ferulic acid was 174.64 °C and the heat of melting was 150.00 J·g-1. The decomposition temperature was 190 °C. Under the condition of nitrogen atmosphere, the DTA-TGA spectrum of ferulic acid was determined by DTG-60 differential thermal-thermogravimetric analyzer, and there was significant weight loss between 190 °C and 260 °C, which confirmed that ferulic acid began at 190 °C in nitrogen atmosphere