[1]ZHANG Rui,Qin Dandan,Wang Hailong,et al.Preparation of SiO2 by sol-gel method[J].Journal of Zhengzhou University (Engineering Science),2006,27(03):119-122.[doi:10.3969/j.issn.1671-6833.2006.03.030]
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Journal of Zhengzhou University (Engineering Science)[ISSN
1671-6833/CN
41-1339/T] Volume:
27卷
Number of periods:
2006年03期
Page number:
119-122
Column:
Public date:
1900-01-01
- Title:
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Preparation of SiO2 by sol-gel method
- Author(s):
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ZHANG Rui; Qin Dandan; Wang Hailong; etc
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- Keywords:
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- CLC:
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- DOI:
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10.3969/j.issn.1671-6833.2006.03.030
- Abstract:
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Ethyl orthosilicate (TEOS) is used as the main raw material, ethanol as solvent, hydrochloric acid or ammonia as catalyst to prepare silicate gel. The mechanism of sol-gel reaction and the effects of catalyst, water, solvent and reaction temperature on gelling time, viscosity and structure of gel were discussed. The two-step Sol-Gel method of first acidic and then alkaline can greatly shorten the gelling time.