<div> <br /> </div> <div>Study on the process conditions of bisphenolic acid synthesis</div>

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Study on the process conditions of bisphenolic acid synthesis

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[1]Fang Shuqi,QIU Jianhua,Zhang Jianjian,et al.Study on the process conditions of bisphenolic acid synthesis[J].Journal of Zhengzhou University (Engineering Science),2006,27(01):106-108.[doi:10.3969/j.issn.1671-6833.2006.01.026]

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Journal of Zhengzhou University (Engineering Science)[ISSN 1671-6833/CN 41-1339/T] Volume: 27卷 Number of periods: 2006年01期 Page number: 106-108 Column: Public date: 1900-01-01

Title:: Study on the process conditions of bisphenolic acid synthesis

Author(s):: Fang Shuqi; QIU Jianhua; Zhang Jianjian; etc

Keywords:: bisphenolic acid; Levulinic acid; Synthesis process

CLC:: -

DOI:: 10.3969/j.issn.1671-6833.2006.01.026

Abstract:: Bisphenolic acid was synthesized by condensation reaction using hydrochloric acid as catalyst, thioglycolic acid as cocatalyst, and levulinic acid and phenol as raw materials. The molar ratio of levulinic acid to phenol, the molar ratio of levulinic acid to hydrochloric acid, reaction temperature and time were selected as follows: reaction temperature 9 °C, reaction time 34 h, n(levulinic acid)∶n(phenol)=60∶45, n(levulinic acid)∶n(hydrochloric acid)=1∶4, n(levulinic acid)∶n(hydrochloric acid)=1∶4, and the yield of bisphenolic acid reached 97.1%.

References:: -

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Last Update: 1900-01-01