[1]ZHAN Yuzhong,ZHOU Xiang,HU Bin,et al.Synthesis and Characterization of Copper Hydroxyphosphate[J].Journal of Zhengzhou University (Engineering Science),2010,31(02):79-.
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Journal of Zhengzhou University (Engineering Science)[ISSN
1671-6833/CN
41-1339/T] Volume:
31卷
Number of periods:
2010 No.02
Page number:
79-
Column:
Public date:
2010-02-02
- Title:
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Synthesis and Characterization of Copper Hydroxyphosphate
- Author(s):
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ZHAN Yuzhong; ZHOU Xiang; HU Bin; etc
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School of Chemical and Energy Engineering,Zhengzhou University,Zhengzhou 450001,China
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- Keywords:
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uniform design; copper hydroxyphosphate; hydrothermal synthesis; p-nitrophenol; degradation
- CLC:
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- DOI:
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- Abstract:
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The hydrothermal synthesis of copper hydroxyphosphate is studied by uniform design method.Theproduct synthesed was characterized by XRD,SEM,FTIR and TG—DTA。The optimal synthesis ratio is ethyl·enediamine/phosphoric acid/copper acetate/water(molar ratio)=1/9.5/7.25/399.Under the optimal con—dition,the pure phase of copper hydroxyphosphate can be synthesed reliably.The synthesis time is short andthe crystal size of product is uniform in the case of ultrasonic pretretament for the mixture of raw materials.Thecopper hydroxyphosphate synthesed has very high activity for the catalytic degradation of p-nitrophen01.