[1]ZHANG Rui,Qin Dandan,Wang Hailong,et al.Preparation of SiO2 by sol-gel method[J].Journal of Zhengzhou University (Engineering Science),2006,27(03):119-122.[doi:10.3969/j.issn.1671-6833.2006.03.030]
                                
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                                    Journal of Zhengzhou University (Engineering Science)[ISSN
                                    1671-6833/CN
                                    41-1339/T] Volume:
                                    27
                                    Number of periods:
                                    2006年03期
                                    Page number:
                                    119-122
                                    Column:
                                    
                                    Public date:
                                    1900-01-01
                                
                                
                                    - Title:
 
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                                        Preparation of SiO2 by sol-gel method
 
                                
                                
                                
                                    - Author(s):
 
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ZHANG Rui; Qin Dandan; Wang Hailong; etc
		
				
		
 
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                                    - Keywords:
 
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                                    - DOI:
 
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                                        10.3969/j.issn.1671-6833.2006.03.030
 
                                
                                
                                
                                    - Abstract:
 
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Ethyl orthosilicate (TEOS) is used as the main raw material, ethanol as solvent, hydrochloric acid or ammonia as catalyst to prepare silicate gel. The mechanism of sol-gel reaction and the effects of catalyst, water, solvent and reaction temperature on gelling time, viscosity and structure of gel were discussed. The two-step Sol-Gel method of first acidic and then alkaline can greatly shorten the gelling time.