[1]ZHOU Cairong,Wang Fei,GAO Bin,et al.Research on a new process for the synthesis of trans-1,2-cyclohexanediol[J].Journal of Zhengzhou University (Engineering Science),2003,24(01):32-37.[doi:10.3969/j.issn.1671-6833.2003.01.008]
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Journal of Zhengzhou University (Engineering Science)[ISSN
1671-6833/CN
41-1339/T] Volume:
24卷
Number of periods:
2003年01期
Page number:
32-37
Column:
Public date:
1900-01-01
- Title:
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Research on a new process for the synthesis of trans-1,2-cyclohexanediol
- Author(s):
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ZHOU Cairong; Wang Fei; GAO Bin; etc
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- Keywords:
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- CLC:
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- DOI:
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10.3969/j.issn.1671-6833.2003.01.008
- Abstract:
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According to the molecular structure characteristics of cyclohexene and the basic theory of related unit reactions, a process route for the preparation of 1,2-cyclohexanediol from cyclohexene oxidation by hydrogen peroxide under the condition of acetic acid and acetic anhydride as oxygen carrier was proposed. The influence of material ratio, reaction temperature, reaction time and other factors was investigated by orthogonal test method and single factor experimental method, and the product was extracted by solvent, and the melting point test and infrared spectrometer analysis method were used to confirm that the product of the synthesis reaction was trans-1,2-cyclohexanediol.