[1]朱消非..乙烯基膦酸酯与硝酮的反应研究[J].郑州大学学报(工学版),2013,34(02):25-27.[doi:10.3969/j.issn.1671-6833.2013.02.007]
　ZHU Xiao-fei.Studies on Reactions of Vinylphosphonates with Nitrones[J].Journal of Zhengzhou University (Engineering Science),2013,34(02):25-27.[doi:10.3969/j.issn.1671-6833.2013.02.007]
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乙烯基膦酸酯与硝酮的反应研究()
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《郑州大学学报(工学版)》[ISSN:1671-6833/CN:41-1339/T]

卷:
34卷
期数:
2013年02期
页码:
25-27
栏目:
出版日期:
2013-03-28

文章信息/Info

Title:
Studies on Reactions of Vinylphosphonates with Nitrones
作者:
朱消非.
郑州大学学报编辑部,河南郑州,450001
Author(s):
ZHU Xiao-fei
Editorial Department of Zhengzhou University Journal, Zhengzhou University , Zhengzhou 450001 , China
关键词:
乙烯基膦酸酯;  硝酮;  环加成反应;  四氢异噁唑
Keywords:
vinylphosphonate ;  cycloaddition reactions;  nitrones;  isoxazolindine
分类号:
0621.3+3
DOI:
10.3969/j.issn.1671-6833.2013.02.007
文献标志码:
A
摘要:
研究了乙烯基膦酸酯与硝酮的环加成反应,发现该反应有三个产物,主产物为4-膦酰基-3-芳基-四氢异噁唑,其结构经核磁和元素分析确证；另两个产物的含量经高效液相确定,通过质谱、氢谱比较确定了它们的结构.
Abstract:
Cycloaddition reactions of vinylphosphonates with nitrones were studied.Three products were ob-tained. 4-phosphonyl-3-arylisoxazolidine is main product and its structure was confirmed by ’H NMR and ele-ment analysis. Yield of other products is analysed by HPLC,and their structures are confirmed by ’H NMRand MS.
更新日期/Last Update: 1900-01-01