[1]吴鸣建,张燕,张海艳,等.川藿苷A的NMR数据解析[J].郑州大学学报(工学版),2012,33(01):68.[doi:10.3969/j.issn.1671-6833.2012.01.017]
　WU Mingjian,ZHANG Yan,ZHANG Haiyan,et al.NMR Numerical Analysis of Sutchuenoside A[J].Journal of Zhengzhou University (Engineering Science),2012,33(01):68.[doi:10.3969/j.issn.1671-6833.2012.01.017]
点击复制

川藿苷A的NMR数据解析()
分享到：

《郑州大学学报(工学版)》[ISSN:1671-6833/CN:41-1339/T]

卷:
33
期数:
2012年01期
页码:
68
栏目:
出版日期:
2012-01-10

文章信息/Info

Title:
NMR Numerical Analysis of Sutchuenoside A
作者:
吴鸣建; 张燕; 张海艳; 等.
郑州大学化工与能源学院,河南郑州,450001, 郑州大学化工与能源学院,河南郑州450001;河南省科学院天然产物重点实验室,河南郑州450002, 河南省科学院天然产物重点实验室,河南郑州,450002
Author(s):
WU Mingjian; ZHANG Yan; ZHANG Haiyan; etc;
1. College of Chemical Engineering and Enerky, Zhengzhou University, Zhengzhou 450001, China; 2. Key l.aboratory of Natu.ral Products ,Hensn Academy of Science,Zhengzhou 450002,China
关键词:
NMR;  归属;  2D NMR;  川藿苷A
Keywords:
NMR; assignment; 2D NMR; sutchuenoside A
分类号:
O641
DOI:
10.3969/j.issn.1671-6833.2012.01.017
摘要:
用NMR数据解析方法对黄酮醇苷类化合物川藿苷A(Sutchuenoside A)的结构进行研究.应用1H、13C MNR、DEPT一维NMR技术和1H-1H COSY、HSQC、HMBC二维NMR技术对其进行检测.使川藿苷A所有的1H和13C NMR数据得到了详细解析和全归属,并进一步确证了其结构.为黄酮醇苷类化合物的结构鉴定提供了可靠的NMR数据解析方法和依据,也为该类化合物的深入研究和应用提供了重要的结构信息.
Abstract:
Sutchuenoside A, one of the flavonol glyeosides, was studied using the NMR data analysis methodand was detected through 1D (1H,13C NMR and DEPT) and 2D NMR (1H-1H COSY,HSQC, and HMBC)techniques. The results show that the ’H and ’"’C NMR spectra are completely analyzed and assigned, and thestructures of sutchuenoside A are further identified. This research provided not only NMR data analysis meth.ods and evidences, but also structures information for the structures identification of flavonol glycosides.

相似文献/References:

[1]李慧,杨宇..磷酰基吡咯/氨基酸缀合物的合成及结构表征[J].郑州大学学报(工学版),2010,31(04):108.[doi:10.3969/j.issn.1671-6833.2010.04.027]
[2]赵天增,张海艳,董建军,等.苦皮素B的NMR数据解析及其化学结构[J].郑州大学学报(工学版),2012,33(06):96.[doi:10.3969/j.issn.1671-6833.2012.06.023]
　ZHAO Tianzeng,ZHANG Haiyan,DONG Jianjun.NMR Study on Angulatin B[J].Journal of Zhengzhou University (Engineering Science),2012,33(01):96.[doi:10.3969/j.issn.1671-6833.2012.06.023]
[3]张海艳,康建勋,董建军,等.朝藿定C的NMR数据解析[J].郑州大学学报(工学版),2013,34(04):94.[doi:10.3969/j.issn.1671-6833.2013.04.022]
　CAO Guo-xi,HU He-fang,GAN Fu-xi.Study on the Optical Properties of Fluorophosphate Glass[J].Journal of Zhengzhou University (Engineering Science),2013,34(01):94.[doi:10.3969/j.issn.1671-6833.2013.04.022]

更新日期/Last Update: 1900-01-01