[1]周彩荣,王晓松,王海峰..山茱萸果核油提取工艺优化及其成分的研究[J].郑州大学学报(工学版),2013,34(03):30-33.[doi:10.3969/j.issn.1671-6833.2013.03.008]
　ZHOUCairong,WANG Xiaosong,WANG Haifeng.Optimization onExtracting the OrganicSubstances from theKernel of Cornus OfficnalisandAnalysis ofIts Ingredients[J].Journal of Zhengzhou University (Engineering Science),2013,34(03):30-33.[doi:10.3969/j.issn.1671-6833.2013.03.008]
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山茱萸果核油提取工艺优化及其成分的研究()
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《郑州大学学报(工学版)》[ISSN:1671-6833/CN:41-1339/T]

卷:
34卷
期数:
2013年03期
页码:
30-33
栏目:
出版日期:
2013-05-31

文章信息/Info

Title:
Optimization onExtracting the OrganicSubstances from theKernel of Cornus OfficnalisandAnalysis ofIts Ingredients
作者:
周彩荣; 王晓松; 王海峰.
郑州大学化工与能源学院,河南郑州,450001, 郑州大学化工与能源学院,河南郑州,450001, 郑州大学化工与能源学院,河南郑州,450001
Author(s):
ZHOUCai—rong; WANG Xiao—song; WANG Hai—feng
School ofChemical Engineeringand Energy，ZhengzhouUniversity，Zhengzhou450001，China
关键词:
山茱萸;  微波处理;  气相色谱-质谱联用技术
Keywords:
comus officnalis; microwave treatment; GC—MS
分类号:
Q914.1：$58
DOI:
10.3969/j.issn.1671-6833.2013.03.008
文献标志码:
A
摘要:
以山莱萸果核油的提取率为考察指标,对经微波处理的山茱萸果核进行索氏提取,用单因素试验和均匀设计试验法确定提取工艺条件,结果表明,以微波处理6 min的山茱萸果核粉末为原料,丙酮作为提取溶剂,较佳的提取工艺条件为:水浴温度为70.5℃、提取时间为75 min、液固比为12 mL/g.同时,用GC-MS分析鉴定其提取物的主要成分为亚油酸、棕榈酸、油酸及其相关酯类,为山茱萸果核有效成分的开发利用提供了依据.
Abstract:
Taking the extraction rate as the indexes，the optimal extraction processing conditionswereexplored by the single—factor experimentand the uniform design experiment．The kernel of cornus officnalis wastreated 6minunder the condition ofmicrowave radiation before extraction process wasdone by acetone as the extrac．tion solvent．The optimum conditions werefound to be water—bath temperature of 70．5℃．extracting time of 75min andliquid—solid ratio of 12 mL／g．Thecomponentsextractedweremainly linoleic acid，oleicacid，pal．mitic acid，etc．byGC—MS．The results provide reference for exploiting and utilizting active ingredients for the kernel ofcomus omcnalis．

参考文献/References:

[1]DUWei—feng，CAI Hao，WANG Ming—yan，et a1．Simultaneous determination of six active components in crude and processed fructuscorni by high performance liquid chromatography[J]．Journal of Pharmaceutical andBiom edical Analysis，2008，48(1)：194—197．

更新日期/Last Update: 1900-01-01