[1]张翔,魏浩栋,姚纪蕾,等.单分散尺寸可控的聚苯乙烯微球的制备[J].郑州大学学报(工学版),2014,35(05):105-108.[doi:10.3969/j.issn.1671 -6833.2014.05.024]
　ZHANG Xiang,WEI Haodong,YA0 Jilei.Preparation of Monodisperse Size-controlled Polystyrene Microspheres by Dispersion Polymerization[J].Journal of Zhengzhou University (Engineering Science),2014,35(05):105-108.[doi:10.3969/j.issn.1671 -6833.2014.05.024]
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单分散尺寸可控的聚苯乙烯微球的制备()
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《郑州大学学报(工学版)》[ISSN:1671-6833/CN:41-1339/T]

卷:
35卷
期数:
2014年05期
页码:
105-108
栏目:
出版日期:
2014-09-30

文章信息/Info

Title:
Preparation of Monodisperse Size-controlled Polystyrene Microspheres by Dispersion Polymerization
作者:
张翔; 魏浩栋; 姚纪蕾; 张冰
Author(s):
ZHANG Xiang; WEI Haodong; YA0 Jilei
School of Chemical Engineering and Energy, Zhengzhou University, Zhengzhou 450001 ,China
Keywords:
polyslyrene mierosphere ;  dispersion polymerization;  monodisperse;  size distribution
分类号:
TQ317
DOI:
10.3969/j.issn.1671 -6833.2014.05.024
文献标志码:
A
Abstract:
Monodisperse size-controlled polystyrene mierospheres were prepared by dispersion polymerizationof styrene in ethanol dispersion medium, using PVP as a stabilizer and AlBN as the initiator. The inlueneefaclors, such as monomer coneentration , stabilizer coneeniralion , iniliator eoneentration and reaction temperature on the size and size distribution were invesligated. The morphology and size of PSt mierospheres was charaeterized by SEM , partiele size analyzer and oplieal mieroseope. And the Fourier transorm infrared ( FTlR )spectra of PSt mierospheres were also reeorded by a FTlR speelrometer. The results showed that monodispersePSt mierospheres in the size of 3.55 pm with smooth surlaee were prepared when the monomer coneentration is22%, slabilizer PVP is 0.65% , iniliator AlBN is 0.32% and reaelion temperalure is 70 ℃.
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