[1]詹予忠,董贺新,董佳佳,等.SAPO-56分子筛的晶化区研究[J].郑州大学学报(工学版),2016,37(03):32.[doi:10.13705/ j.issn.1671 -6833.2016.03.007]
　ZHAN Yuzhong,DONG Hexin,DONG Jiajia,et al.Study on crystallization area of SAPO-56 molecular sieve[J].Journal of Zhengzhou University (Engineering Science),2016,37(03):32.[doi:10.13705/ j.issn.1671 -6833.2016.03.007]
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SAPO-56分子筛的晶化区研究()
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《郑州大学学报(工学版)》[ISSN:1671-6833/CN:41-1339/T]

卷:
37卷
期数:
2016年03期
页码:
32
栏目:
出版日期:
2016-05-10

文章信息/Info

Title:
Study on crystallization area of SAPO-56 molecular sieve
作者:
詹予忠; 董贺新; 董佳佳; 宋孟璐; 韩丽; 陈宜俍
郑州大学化工与能源学院,河南郑州450001
Author(s):
ZHAN Yuzhong; DONG Hexin; DONG Jiajia; SONG Menglu ; HAN Li
School of Chemical kngineering and Energy ，Zhengzhou Unversity , Zhengzhou 430001 ,Chna
关键词:
磷酸硅铝分子筛; 水热合成; 晶化区; 模板剂
Keywords:
silicoalumino-phosphate molecular sieve;  hydrothermal synthesis; crystallization area; template agent
DOI:
10.13705/ j.issn.1671 -6833.2016.03.007
文献标志码:
A
摘要:
以N,N,N’,N’-四甲基-1,6-己二胺(TMHD)为模板剂、拟薄水铝石为铝源、白炭黑为硅源、磷酸为磷源,采用静态水热法合成SAPO-56分子筛.产物晶相和结晶度采用XRD确定,考察原料配比对分子筛合成的影响,获得了合成SAPO-56分子筛的晶化区.结果表明,可合成SAPO-56分子筛的摩尔比范围大致为:0.16
Abstract:
SAP0-56 molecular sieve was synthesized hydrothermally using N,N,N’,N’,-tetramehtyl-hexane-1,6-diamine (TMHD) as template agent,pseudo-boehmite as aluminum source,white carbon black as sili-con source,and phosphate acid as phosphorus source.The crystal phase and crystallinity of product were i-dentified by XRD. The influence of synthetic conditions on the molecular sieves was studied and the crystalli-zation area of SAP0-56 molecular sieve was obtained. The results showed that the crystallization area of SAPO-56 was n(0.16
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